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Kind: captions Language: en nitrogen is everywhere it's a fundamental building block of life it makes up 78 of the atmosphere and it's in these tiny micro bubbles in my starbucks nitro cold brew and yes this episode is sponsored by starbucks they challenged me to liquify nitrogen out of the air and that's what i'm going to be doing in this video but first i'm going to try nitro cold brew for the first time it's subtly sweet without having to add sugar and obviously it's cold and frothy and i'm gonna explain why nitrogen makes this possible but first i'm gonna try to liquefy some nitrogen for myself out of this atmosphere come on let's go okay in order to make liquid nitrogen we need a way to make the air really cold and to do that i'm going to use this cryo cooler so essentially what's inside here is a cylinder of helium and a couple pistons so there's a piston that compresses the helium down into this section and when it does that it makes that gas really hot and so that heat gets ejected to the surroundings through this heat sink then the helium is expanded down in here and as that happens it gets really cold so it absorbs the heat from the surroundings so this is the part of the cryo cooler that is going to get down to less than minus 200 degrees celsius so cryogenic temperatures this is the place where we can really liquefy some gas so i want to put this to the test and first do a sort of simple proof of concept and make sure that this is working and just try to liquefy air liquefy the air in this room this is alan pan allen is handier with tools than i am so uh brought him in to help me make this happen how should people know you alan like what do you get into what's your thing uh i'm a failed mythbuster and also i have a youtube channel called sufficiently advanced you may know alan from his creations and relevant to this project shooting liquid nitrogen from his hands i'm definitely breaking your drill by the way that plastic is coming right i see that did i measure this correctly let's see does it go in and stop right there oh my god look at that perfect so now let's turn it on and you can listen you can hear it turn on oh the pump is starting it's purring this is the moment of truth been running the crowd cooler for about four hours hopefully getting some liquid air in there i bet you 50 bucks there's at least 50 milliliters of liquid air in there 50 milliliters sir that's not even that much it isn't even that much i'll be amazed i'll be amazed if it happens oh that that's 50 milliliters right there i bring you a 50 milliliter do beaker feel any sloshing i hear something i hear something i hear something in your liquid we have made liquid air that's how much have we made 50 milliliters is that how much we make of liquid air oh dude that's 50 milliliters of liquid air i know it doesn't look like much but to make 50 milliliters of liquid air we needed to condense around 35 liters of air from the room what's funny to me is i've done a lot of experiments with liquid nitrogen but this feels like the most precious liquefied gas that i've ever had because we made it ourselves there was more than 50 ml i know we didn't shake on it but you definitely owe me 50 i definitely do because that's impressive from just a few hours you know running it for the first time liquid oxygen is paramagnetic which means it's attracted to permanent magnets i'm going to use this effect to try to extract some liquid oxygen something oh dude you got it you got some see that droplet at the end of the magnets to make sure it really was liquid oxygen we tested how it affected a flame so that's for sure oxygen that is liquid oxygen you can see how the matchstick reignites with the liquid oxygen and the flame spreads towards the higher concentration of oxygen [Applause] oh [Applause] there you go we have made liquid air next step remove the oxygen and just make liquid nitrogen okay it is day two and time to scale up we are moving the crowd cooler to a bigger stand should i just go yeah go for it i'm putting a lot of sawdust into your into your carpet i'm sorry it's okay to make pure nitrogen we need pressurized air so i've got an air compressor here in the garage the pressure of this compressor is about 10 atmospheres so i'm going to pressurize this line here now the first thing we got in the line is a filter to remove water vapor now to get pure nitrogen this is the key component it is a nitrogen membrane and what it actually contains is a bunch of hollow polymer fibers and so we supply compressed air in this end and all of the gas molecules try to diffuse out of those fibers because of that high pressure but these polymer fibers are made out of a material that is selectively permeable it allows oxygen and carbon dioxide and water vapor to diffuse out much faster than nitrogen and so those gases actually come out preferentially through these holes so what you're left with at the end is a high concentration of nitrogen and to get the highest purity what you need to do is have a very high pressure and a slow flow rate because that gives a lot of time for those other gases to escape whoa i don't know about this gauge so what i want to call and watch is how long it takes to increase the pressure in the tank well we worked it out yesterday and we figured out if it takes six minutes to fill the tank at 100 psi then we've got 98 pure nitrogen cool perfect right but we just have to be very slow with this tank filling and i don't know if we are that slow we're going to try to check the oxygen levels that have come through this membrane let's put some money on it how about 50 bucks as the oxygen is less than 5 yeah are you gonna bet that because i will easily take that back yeah all right i don't think this went very well because that was the first filling of the tank so we weren't high pressure going through the membrane so i don't think it's gonna be i think we're good 95 percent nitrogen 95 nitrogen so this meter measures oxygen so we're looking for a number less than five percent which i suspect we will not see oh can he oh it's it's going away come on five percent for oh there it is whoa here we go 99 99 not over 99 percent 99.2 99.3 i am shocked there's no oxygen in this air baby it's all nitrogen 99.5 i am so shocked right now so we're at 50 bucks for the liquid air bet we're at 50 bucks yeah you just found yourself 100 bucks look at that 99.7 percent nitrogen this is insane and you can understand why there would be an alarm if you were in a room with 1.3 oxygen yeah i knew it i told you you knew this would hurt you yes okay so we've achieved i guess the second part of this which is isolating nitrogen from the atmosphere and now we just have to get it super cold what we gotta do is we gotta put this thing here for better insulation we scaled up to a doer that's impressive kind of sci-fi janky garage sci-fi kind of a look go ahead and lower that it'll just squish right on i hope i mean that's that's sealed you know i think uh honestly we could just turn it on and see if it works at this point start bleeding some nitrogen in there so that when the nitrogen goes in there it'll push out any remaining air that's still in the tank i'm going to switch on the variac which powers up the crow cooler the other thing i need is the fan yes this is the fan i'm gonna plug that in that's a cooling fan of the grout cooler we're up to eight watts okay i have been running the nitrogen setup for about three hours and my concern because the temperature on the thermocouple never got very low was that i wasn't actually making any liquid nitrogen so i've stopped the test and i just want to see whether or not there is anything in here it doesn't sound like it nothing huh what i think could be part of the problem i was putting nitrogen possibly at a rate that's too high so this is effectively nitrogen coming in at room temperature and i wonder if it was just too warm for it to ever reach the liquefying temperature right here at the end of the uh the cold finger of the crowd cooler so i feel like i need a slower flow rate maybe a better way to introduce the nitrogen into the dewar not as easy as i'd hoped okay my plan is to go with a smaller flask something like this and we're gonna use its lid to make a nice tight seal except we're gonna cut a hole through the top i think it's good enough for this cold finger all right then we're gonna try to drill a hole in the side uh for the supply of nitrogen we need to make nice tight seals around both of those things so that is gonna be the challenge this is the uh kind of the new design here that we've got i feel like it's pretty good i think it's gonna work i think you're gonna wake up and there's gonna be like a nitrogen in there i bet you a hundred and sixty dollars that there is liquid nitrogen in there i don't know if i'll take that out i'm going to turn down the cryo cooler and let's see what we got it looks cold yeah there's definitely some condensation so there's something cold in there what do you see oh there's luminite there's like this much that's liquid nitrogen we have some liquid nitrogen out of the air that was so much effort so what do you do with homemade liquid nitrogen well make homemade ice cream just a bit of cream and sugar and then the liquid nitrogen the most precious liquid nitrogen i've ever had is it enough to make ice cream come have a look have a look that is delicious by freezing everything so fast because it is minus 196 celsius you get really small ice crystals and so that gives the ice cream a really smooth flavor smooth texture in a lot of stores starbucks ii generates nitrogen just out of the air because why not it's an available resource they purify it and then infuse it in line into the drink creating millions of those tiny bubbles that gives it its unique texture so nitrogen bubbles are much smaller than the bubbles you're normally used to the carbon dioxide bubbles that you'd find in soda and that gives this a sort of creamier texture the other nice thing about nitrogen is that it's totally inert so it doesn't react with the drink co2 reacts with water creating some acid which you might like in soda you might want a little bit of a sour tangy flavor but you don't want that in coffee hence the nitrogen one thing i found really interesting when they were pouring this nitrocol brew is that you can actually see bubbles coming down on the sides of the glass and that's strange because these bubbles are obviously less dense than the coffee they should be rising up to the surface so why are they doing that well the answer is the nitrogen bubbles are rising up to the surface a lot in the center of the drink and so that actually creates a current that pushes them down around the outside and so that's why you see those bubbles cascading down at the beginning when you're pouring the nitro cold brew so there you have it nitrogen is everywhere and useful for lots of things if you want to try out a nitro cold brew i'll put a link to order it down in the description and thanks for watching you
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